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Saturday, July 26, 2025

Utica-Point Pleasant Evaluations Via XRF Chemostratigraphy and Sequence Stratigraphy


   

     The Point Pleasant member of the Utica Shale is a mixed siliciclastic and carbonate sequence, where it produces oil and gas in the Appalachian Basin. The Utica above it is a siliciclastic mudstone, while the Point Pleasant is more of a calcareous mudstone. One key to optimizing production in the formation is to target structural settings in the Ohio sub-basin where the highest amounts of organic matter and resulting organic porosity are preserved. Typically, this is in structurally low topographic settings far enough below wave base to enable higher preservation.

     The use of X-Ray Fluorescence (XRF) in determining chemostratigraphy is well-documented. It can be used to analyze cores and drill cuttings to define ideal zones for targeting in horizontal wells, for noting stratigraphic differences over an area and continuity of beds, and to inform geosteering if done in real-time. As noted in a 2021 Master’s Thesis by Barbara Kemeh:

“…chemostratigraphy reflects changes in depositional and facies characteristics of the Utica shale and Point Pleasant Formation.”

     I am utilizing Kemeh’s 2021 Master’s Thesis and Zachary Fernandez’s 2023 Master’s Thesis as the main sources in this post.

      Also from Kemeh’s thesis:

“For this study, two cores were analyzed using a handheld x-ray fluorescence (HH-XRF) spectrometer along with core descriptions, x-ray diffraction (XRD) and total organic carbon (TOC) data to interpret the depositional environment. Hierarchical clustering technique was used to identify five chemofacies which reflect the geochemical variability present in both cores. Six chemozones were identified and correlated using the chemofacies coupled with stratigraphic plots of selected major elements, trace metals and TOC. Detrital influx analysis revealed that the Utica-Point Pleasant interval in both cores were deposited in different water depths resulting in different amounts of terrigenous input. Paleoredox conditions revealed the Farley core was deposited in oxygenated bottom waters which account for the depletion of trace metals throughout the core. In the Tracker core, analysis showed that bottom-water conditions at the time of deposition varied between anoxic and euxinic. The Tracker core shares similar bottom-water conditions present in the Sebree Trough in Kentucky and is believed to have been deposited in an extension of the trough into northeast Ohio. The Farley core appears to have been deposited outside this trough and likely in the Utica-Point Pleasant basin. Overall the study supports the existence of different depocenters across the area with different conditions at the time of deposition.”

     It is important to know paleoredox conditions since they affect the preservation of organic matter beds. Chemostratigraphy can be used to help determine redox conditions, water depth during deposition, as well as the percentage of terrigenous detrital sediment delivered to the seafloor vs. marine sediments via carbonate accumulation.

     Kemeh begins her thesis with the note that two-thirds of the sedimentary rock record consists of mudstones. She also notes the variability between mudstones and within mudstones, often at centimeter scale. Fine-grained rocks like shales can often result in ‘condensed intervals’, which refer to thin beds that cover long time periods during mostly very slow deposition in deeper waters. 






     The definition of a condensed interval given by Wikipedia is as follows:

In sequence stratigraphy. condensed sections are strata that are thin, yet span a large time interval. They are associated with the maximum flooding surfaces, represented by sedimentary intervals deposited during the maximum marine transgression.”

    Zachary Fernandez, in his 2023 Master’s Thesis, noted that in sequence stratigraphy, the condensed intervals are associated with the end of the Transgressive Systems Tract (TST) and capped by the Maximum Flooding Surface (MFS). The condensed interval is thus the interval with the least amount of influx of terrigenous sediment due to high sea level. This leads to optimal preservation of organic matter. First, the chemo facies are identified from the elemental content, then they are paired with sequence stratigraphy depositional systems tracts.

     Below, Kemeh explores the reasons for variability. She also explains how different elements can be proxies for local environmental conditions during deposition. Ti, Zr, K, and Al can indicate detritus deposited during sea level transgression and regression. Ca, Mg, and Sr are associated with carbonate accumulation. Al and K indicate feldspars and clay. “The combined use of Mo, V, and U is used in distinguishing suboxic environments from anoxic-euxinic ones.”

The major influences on variability in mudrocks include tectonic setting, water depth, oxygenation, climate, eustasy, and detrital influx which control composition, fabric, and texture. Thus, different lithofacies are produced from changing transport and depositional processes, while mineralogical and total organic carbon (TOC) variations can be attributed to proximity to sediment source.”

     Zachary Fernandez noted chemostratigraphic proxies as follows:

“…proxies for terrigenous sedimentation (Ti, Zr and Rb), marine sedimentation (Ca and Sr), clay sedimentation (Al and K), upwelling (P), pyrite minerals (Fe and S) and biogenic quartz (Si/Al)

     Regarding the use of chemostratigraphy, Kemeh notes:

Chemostratigraphy relies on identifying variations in element concentrations through an interval and using these changes to develop a stratigraphic characterization that is based on changes in geological features, such as paleoclimate (Pearce et al., 2005b, Ratcliffe et al., 2010) and provenance (Ratcliffe et al., 2007, Wright et al., 2010).”

     Kemeh utilized two cores for the XRF study: The Tracker core from Portage County, Ohio, and the Farley core from Washington County, Ohio. She characterizes the study below:

The focus of the study was to establish chemostratigraphic correlations and paleoenvironment proxies, such as water bottom oxygen levels, based on trace metal concentrations within the Utica shale and Point Pleasant Formation across Ohio which will help formally characterize the Utica shale within the state.”   

     Below, she gives elemental proxies, a cross-sectional model of deposition showing wave base and positions of the two cores, and a relative sea level curve.









     Fernandez’s study analyzed 31 wells from eight counties in eastern Ohio. He used an Olympus Delta Pro Handheld X-ray Fluorescence Spectrometer (pXRF), which is less accurate than a tabletop XRF but adequate for determining the relative abundance of elements. Fernandez recognized three chemofacies beginning at the base of the Point Pleasant.

“Chemofacies 1 has the lowest clay proxies of the entire section. It has the highest indicators of upwelling. Redox proxies are low with a minor increase at the top of the chemofacies. Marine sedimentation is variable, yet overall high. Terrigenous sedimentation is variable, yet overall low. Biogenic quartz steadily increases up section.”

Chemofacies 2 is dominated by terrigenous sedimentation.

Clay proxies are high and steady. Redox proxies are intermediate and steady. Marine sedimentation has significantly dropped off and it is decreasing further. Lastly, the proxy for biogenic quartz has leveled off. The top of chemofacies 2 is marked by another shift in sedimentation, the decline of biogenic quartz and the rise of redox proxies.”

Chemofacies 3 “has increasing clay proxies. The redox proxies are at their zenith in this chemofacies. Marine sedimentation is rapidly decreasing, and terrigenous sedimentation is rapidly increasing; however, there is some significant variability in this overall sedimentation trend. The final attribute of this chemofacies is that biogenic quartz is steadily decreasing.”

Chemofacies displaying high proxies for marine sedimentation (Ca and Sr) and upwelling (P) are denoted as the Transgressive Systems Tract (TST). The TST may also have a high clay content (Al and K). Chemofacies displaying high proxies for terrigenous sedimentation (Ti, Rb and Zr) and low redox sensitive proxies (Fe and S) are denoted as the Highstand Systems Tract (HST). Finally, chemofacies displaying high terrigenous sedimentation and high redox sensitive elements are denoted as the Lowstand Systems Tract (LST).”

     Chemofacies 3 is where the main oil & gas producing interval is in the Point Pleasant, more specifically, the top of chemofacies 3, where the upper few feet have been interpreted as a condensed interval, as shown below.

















     The cross-section below shows correlation via gamma ray and resistivity logs done by EMF Geoscience. It shows that there are good gamma and resistivity indicators for the top of the condensed interval, which occurs at the top of OPTPL2, as correlated. Below that is a sequence stratigraphy interpretation showing the condensed interval at the maximum flooding surface.  The third graphic below is an isopach map of the CI, which varies from 4 to 13 feet in thickness. Unfortunately, it is not referenced to a geographic map, so it is unclear exactly where the thick is. I was a bit surprised at the variation in thickness, and it makes me wonder about that variation throughout the producing area.





     Fernandez notes:

Isopach maps reveal a unique trend. That the formation thickens to the northeast; however, the CI is thickest in the center of the region. Many of the wells in this study land in the CI hotspot. This interval of core was also the section that was most densely sampled for the TOC analysis. It is apparent that there is significant interest in this interpreted CI.”




     Kemeh notes that the organic-rich facies in the Point Pleasant have roughly 40% to 60% carbonate content, with TOC ranging from 3% to 8% (average 4%–5%). She used the elemental ratio of Si/Al to determine if quartz was detrital or biogenic.

     Kemeh distinguished five chemofacies, including parts of the Trenton Limestone. She grouped the chemofacies into chemozones of certain sequences. She notes that in the Tracker core, the rocks were deposited in more anoxic waters below wave base. The Farley core shows more storm deposits and more oxygenated waters, often above wave base.  










     Kemeh’s conclusions are given below:

1) Chemostratigraphy is a useful method of distinguishing between the formations in the Utica shale Play in Ohio.

2) Raw elemental curves allow identification of changes in mineralogy at a finer scale while cluster analysis removes the burden of meaningful pattern identification and correlations across the raw curves by grouping samples based on the degree of similarity to one another.

3) Decreased Ca concentration and increased Al from the Utica-Point Pleasant interval record a shift from the calcareous mudstones of the Point Pleasant to the siliciclastic rich mudstones of the Utica shale.

4) It is assumed that the depositional environment for the Lexington-Utica interval in the Farley core was mostly likely a carbonate shelf to a storm-dominated deep ramp between fair weather and storm base, <131 ft (40 m), frequently disturbed by storm currents. The Trenton-Utica interval in the Tracker core was interpreted to be deep ramp, dominantly below storm wave base in anoxic bottom water, >131 ft (40 m). These different conditions support the existence of separate depocenters across the area.

5)  Bottom conditions of the Tracker Core compared to the Farley core suggests an extension of the Sebree Trough across northeast Ohio, where oceanic conditions allowed for the enrichment of redox sensitive trace metals indicating euxinia to anoxia.  

     Further studies are ongoing. EMF Geoscience is continuing to collect XRF data regarding the condensed interval. According to their website:

EMF Geoscience has purchased a Vanta M Series Handheld XRF and started collecting geochemical data from in-house Point Pleasant cores in September 2023. The primary goal of this Chemostratographic study is to define the Condensed Interval inside the Point Pleasant Formation.”

 

 






References:

 

IDENTIFYING THE POINT PLEASANT FORMATION’S CONDENSED INTERVALS WITH XRF CHEMOSTRATIGRAPHY: A THESIS SUBMITTED TO THE GRADUATE SCHOOL IN PARTIAL FULFILLMENT OF THE REQUIREMENTS FOR THE DEGREE MASTER OF SCIENCE. BY ZACHARY FERNANDES. DR. JEFFRY GRIGSBY – ADVISOR. BALL STATE UNIVERSITY. MUNCIE, INDIANA. May 2023. content

Geochemical Characterization of the Utica Shale Play using XRF-Based Chemostratigraphy in Ohio. Barbara Kemeh and Advisor Julie M. Bloxson. Masters Thesis. Stephen F Austin State University. May 4, 2021. Geochemical Characterization of the Utica Shale Play using XRF-Based Chemostratigraphy in Ohio - Stephen F. Austin State University

Exploration Opportunities North America: Utica – Point Pleasant Shale. Satinder Chopra, Ritesh Kumar Sharma, Hossein Nemati, and James Keay; TGS. GeoExPro. December 10, 2018. Utica - Point Pleasant Shale - GeoExpro

Southeastern Ohio Pt. Pleasant: A Shale Play? Chad Cunningham, presented at Appalachian Geological Society Meeting, Jan. 19, 2016.

Condensed sections. Wikipedia. Condensed sections - Wikipedia

Sequence Stratigraphy and TOC Modeling of the Utica-Point Pleasant Interval in the Middle Appalachian Basin. Taylor McClain. AAPG Datapages/Search and Discovery Article #90262 ©2016, AAPG Division of Professional Affairs, Pittsburgh Playmaker Forum, Pittsburgh, Pennsylvania, April 13, 2016. View PDF

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