Monday, October 30, 2023

Brine Mining: Mineral Extraction Opportunities from Oilfield and Geothermal Brines

 


     Brine mining refers to the extraction of minerals from brines by evaporation and/or precipitation or by chemical, physical and/or electrical separation. Brine mining began with extracting salt from seawater. Potassium is sometimes extracted from the bittern left over from salt precipitation. The seawater bittern solution contains sodium, potassium, magnesium, calcium, chloride, sulfide, iodide, and other ions that precipitate out as compounds, as salts along with the sea salt. Bittern is one of the coagulants used in the production of tofu. It is used in the treatment of some wastewater and to make fertilizer. Epsom salts are another bittern precipitate. Desalination plants process seawater to extract the salts.

     The Chinese began digging brine wells around 500 B.C., some over 330 ft deep. The wells utilized salt-resistant bamboo for derricks, ropes, and casing. Iron wedges pounded the bamboo into the ground by men jumping on a lever.

     A January 2023 paper in Nature Water - Prospects of metal recovery from wastewater and brine – did some technological and economic feasibility analyses of brine and industrial wastewater mining. They concluded that initial concentrations of the minerals in the brine and wastewaters and the cost of each mineral commodity dictates viability. Thus, only certain brines and wastewater will be prospective.  

 

 

Saline Lakes, Shallow Groundwater Brines, Geothermal Brines and Deep Brines in Sedimentary Basins

 

     Brine is also mined from saline lakes that have higher salinity and yield higher concentrations of salts than seawater. The Dead Sea and the Great Salt Lake are examples. Different saline lakes have different chemistries. Shallow groundwater brines are associated with saline lakes or dried-up saline lakes. Deeper geothermal brines may influence the chemistry of shallow groundwater brines. Sodium sulfate, soda ash, salt, colloidal silica, boron, magnesium, calcium, potassium, bromine, zinc, tungsten, and iodine are other extractable minerals and compounds from saline lakes, shallow brines, and deeper geothermal brines. The tables below show some of the main locations, sources, and concentrations of mined brines.

 





    

Lithium Recovery from Ores and Brines

     Lithium is produced from lithium-rich rock from pegmatite deposits such as spodumene and from the extraction of salts from subsurface brines. Some lithium is also expected to be produced from clay. Lithium from rock ore is of higher concentration but is more costly to produce because it requires digging out, crushing, heating, and cooling. Lithium from shallow brines is concentrated through time in evaporated ponds called salars in Chile, Argentina, and Bolivia in an area of the Andes with very little rainfall. Brine is extracted from shallow wells and evaporated in ponds on the surface to concentrate the mineral precipitates. When concentrations reach suitable levels, the mineral salts are taken for further processing. Now there are new methods to extract lithium and other minerals from brines that do not require the very large evaporation ponds.

     The economics of lithium extraction depend on the concentrations of lithium in the brines and ores, the cost of extraction, and the price of lithium. Lithium prices have been high in recent years and demand is expected to stay robust in the years to come as more EVs, grid-scale batteries, and lithium-powered products are built. The downsides of lithium extraction via solar evaporation ponds include the long timelines (18 months), the large amount of required acreage, and the environmental impacts.

     Lithium is further processed into metals. Via an electrolytic cell, lithium chloride (55%) is mixed with potassium chloride (45%). This makes a molten eutectic electrolyte. The combined chemicals increase the conductivity of the lithium and lower the fusion temperature. When fused and electrolyzed at 840 deg F chlorine gas is liberated, and molten lithium rises to the surface. It is collected in cast iron and treated with paraffin to prevent oxidation. It takes about 5.3 times as much lithium carbonate to make the same amount of lithium metal.

 

 













Direct Lithium Extraction (DLE) from Brines

     The methods of lithium production in the salars and solar evaporation ponds in South America are not applicable to other places due to space requirements and environmental degradation. The South American high deserts are not populated, have a low amount of flora and fauna, and much of the groundwater (the brine) is already naturally contaminated and unsuitable for drinking. Direct lithium extraction (DLE) has far less environmental impact and space requirements. The DLE process relies on filters, membranes, ceramic beads, and other equipment to extract lithium and other minerals. The post-extraction water is pumped into wastewater injection wells nearby. The process resembles a wastewater treatment plant.






     An article in Civil Engineering Magazine describes it as follows: “Depending on a particular brine’s geochemistry, various pretreatment steps are used to remove solids, hydrogen sulfide, and other contaminants. Adsorption, ion exchange, and solvent extraction are among the most common methods under development to extract lithium directly from brine.” DLE methods are applicable as well to the South American brines traditionally extracted with solar evaporation ponds and offer a way for those companies to reduce their environmental footprint. Goldman Sachs thinks DLE will be adopted in many of those operations in the 2025-2030 timeframe. Their market report from late April 2023 suggests that costs are comparable between solar evaporation ponds and DLE. DLE requires higher upfront costs but recovers much higher percentages of lithium. The ability to eliminate many of the environmental downsides at comparable costs makes widespread adoption likely.

     A paper in Nature Reviews Earth & Environment - Environmental impact of direct lithium extraction from brines – noted that many environmental impact studies of DLE thus far have not been performed on real brines. Thus, there may be some pre-processing issues for different brine chemistries. Those often require heat energy and have emissions. Environmental impact studies of DLE methods need to consider the use of heat, pH adjustment, and other energy and water inputs when doing a lifecycle analysis for each method. For instance, methods requiring high water inputs would not be environmentally sound in arid areas. They would also be less cost-effective.  

     There are three main DLE methods in operation and two more in development. Those in operation are adsorption, ion exchange, and solvent extraction. Those in development are membrane separation and precipitants. High lithium demand and prices and new government incentives for domestic critical minerals production in the U.S. have spurred new pilot and production projects for DLE technologies.

     Adsorption is the most developed DLE method globally. This method is used in many other industries as well. One of the advantages of adsorption is that it uses water to yield lithium chloride and soda ash to yield lithium carbonate rather than using reagents (acids). It produces less waste and is efficient as it extracts over 90% of the lithium. It does have high upfront costs, some process contamination issues, can have high operating costs, and may require additional heat energy.

     According to Goldman Sachs: “Ion exchange systems separate ionic contaminants from solution through a physicochemical process where undesirable ions are replaced by other ions of the same electrical charge. Essentially, the ion-exchange material acts as a sieve with an adjusted porosity that only allows lithium (and hydrogen) ions to pass through, where the ion-sieve can then be washed with an acidic solution promoting the replacement of lithium ions with hydrogen ions. Lithium recovery by ion exchange can change with a simple adjustment in pH, temperature, or stream composition (though the same goes for other lithium extraction methods), but researchers also believe this method can recover ~90% of the lithium present.” Several of the Salton Sea projects as well as Standard Lithium’s Smackover projects plan to use ion exchange DLE with some expected to commence operation in 2024. Advantages of ion exchange include simplicity of the process, low chance of process contamination, high capacity, ability to process low-concentration brines, low energy and water consumption, and likelihood of continuous operation. The downsides include high acid and base input requirements with accompanying risks, high upfront costs, and some components vulnerable to acid degradation.

     Solvent extraction utilizes a physical means or a chemical combination of a solvent (often kerosene) and an extractant to separate out the lithium since the extractant will select lithium over sodium and magnesium. Solvent extraction can also be used as a post-DLE step to “polish” the lithium closer to battery quality. The method has a high recovery rate, and low operating costs, and it eliminates one of the steps in the other two methods. The downsides of the method are that it is not applicable to brines with lower lithium concentrations, or those with high concentrations of magnesium and calcium (which would require preprocessing). The solvents are also a fire risk with high temperature brines, have corrosion issues, and environmental transport and disposal issues. It is also an expensive process.

     Membrane separation utilizes membranes to separate lithium and magnesium ions and may utilize one of the following to induce the process: pressurized nanofiltration, electric field(electrodialysis), or thermal gradient. The process is efficient with low environmental impact but is not applicable to brines with high sodium or potassium concentrations. It is a water-intensive process that is also expensive.

     An interesting new membrane separation method involves using 12-Crown-4–functionalized polymer membranes in coordination with ion binding sites to select for lithium chloride over sodium chloride. Imbuing the polymers with interactants gives them the ability to foster the ion transport that separates the lithium out. The sodium ions bind to the crown ether enough to slow them down so the lithium ions travel faster through the polymer. The researchers from the University of Texas at Austin and the University of California, Santa Barbara think that this is a promising method for extracting from oilfield-produced water.  The table below from Goldman Sachs compares the different brine extraction methods.    

 









 

The Upper Jurassic Smackover Formation Deep Sedimentary Basin Lithium Brine Play

 

     Thus far, the best brine lithium concentrations in the U.S. have been found in the Upper Jurassic Smackover Formation which is distributed deep in the subsurface along the Gulf Coast Basin from Eastern Texas to Western Florida. It is a deep sedimentary basin brine developed in the past as a very productive oil & gas reservoir in Mississippi, Louisiana, Alabama, and Southern Arkansas. The brine production comes from zones about 7500-8500ft below the surface in Southern Arkansas. A company called Standard Lithium has been focusing on lithium extraction from Smackover brines for a few years now. It is probably one of the best lithium brines outside of Chile and Argentina, according to Standard Lithium.

 








     Just a few weeks ago on October 10, 2023, Standard Lithium announced that from a newly drilled well in East Texas they achieved the highest brine concentration in North America at 663mg/L which is comparable to the South American brines. Two samples were taken from the Upper Smackover with the avg. lithium concentration at 638mg/L. Just a few days ago they reported that a sample from another well measured lithium at 806mg/L which broke the record from a few weeks ago. The average overall for their East Texas field is 644mg/L. In addition to lithium, Standard’s East Texas wells tested at economically viable concentrations of potassium and bromine as well. Lithium concentrations as high as 597mg/L have been found in Southwest Arkansas.

 





     The Smackover formation is limestone, often sucrosic, and locally dolomitized. It overlies the Norphlet formation and more importantly the Louann Salt formation. The Louann Salt is the source of the minerals that migrated via faults through the Norphlet formation into the Smackover. Authors Eva P. Moldovanyi and Lynn M. Walter in a 1992 AAPG Bulletin article note that their regionally extensive database of Smackover water geochemistry shows that heterogeneities in Smackover water geochemistry occur along faults due to upward migration of hotter fluids. “One of the most pronounced heterogeneities in water chemistry is an H2S-rich anomaly in the center of the shelf. Enrichments in H2S are accompanied by large increases in alkali elements (Li, K, and Rb) and B, which could be produced by higher temperature diagenesis of clay minerals and feldspars in deeper seated siliciclastic strata.” They also note that bromide and chloride, concentrated by seawater evaporation, were further enriched by halite dissolution followed by expulsion of meteoric waters along fault systems. Looking at Standard Lithium’s Li concentration numbers in Southwest Arkansas on a map suggests that while Li concentrations vary quite a bit, they could be contour mapped and compared with structural geology to help determine trends. In a 2018 thesis, Pamela Joy Daitch utilized the U.S. Geological Survey National Produced Waters Geochemical Database to identify lithium-rich brine from wells across the U.S. She found that the Smackover formation was by and far the main lithium-rich formation brine in the U.S. Based on financial analysis she also determined that the best way to develop the Smackover was to drill standalone brine wells where concentrations are the highest. This is how Standard Lithium is approaching the play. She also noted an economic cutoff concentration for lithium production of about 70mg/L. This, of course, will vary depending on lithium prices and extraction innovations. Some of the lithium projects in Alberta, Canada are at the low end of profitability with concentrations of about 75mg/L.

 

 

The Smackover Bromine Play

 

     The Smackover formation brine has long been a major source of bromine. Bromine production in Southern Arkansas began in 1957. According to the Arkansas Dept. of Energy & Environment: “Since 2007, all US bromine has been produced in southern Arkansas. In 2013, 28% of the global bromine production (225,000 tonnes) in Arkansas made the United States the second-largest producer of bromine, after Israel. At an advertised price of US$3.50 to US$3.90 per kg, the 2013 Arkansas production would have a value of roughly US$800 million.” Fire retardants are the major use of Arkansas bromines, making up about half of the production. Other uses include insect and fungus sprays, anti-knock compounds for leaded gasoline, disinfectants, photographic preparations and chemicals, solvents, water-treatment compounds, dyes, insulating foam, hair-care products, pharmaceuticals, energy storage, mercury emissions reduction, reinforcing rubber materials, and oil well-drilling fluids. Bromine is a highly corrosive liquid. It is harmful if it contacts human skin and breathing its vapors is harmful, so safety precautions are in place at processing plants. Albemarle Corporation and Chemtura are the two biggest bromine producers in South Arkansas.

 

 



 

The Salton Sea Geothermal Brines Lithium Play in Southern California

 

     In California, the geothermal brines below the evaporating Salton Sea are a great source of lithium and other minerals. The hot brines are already being circulated to the surface in geothermal wells to power the steam turbines of the geothermal plants. Brine production rates are high in the Salton Sea. The high flow rates associated with the geothermal wells mean processing rates have to be high to keep up. This is challenging. Many DLE projects are ramping up in the Salton Sea play. Investors include Energy ventures by Bill Gates and Jeff Bezos, Warren Buffet’s Berkshire Hathaway, the U.S. DOE, and automaker Stellantis. The biggest players in the Salton Sea DLE Projects are Berkshire Hathaway Energy, EnergySource Minerals, and Controlled Thermal Resources (CTR).

     The Salton Sea is one focus for the U.S. ramp-up of domestic critical minerals production, deemed as necessary to reduce dependence on China and to eventually ease supply chain issues. Typically, geothermal energy powers mineral extraction, keeping emissions low. Some CO2 is released in the steam that surfaces in the course of geothermal energy production.

     As of 2022, there were 11 geothermal power plants in the Salton Sea area, also now known as Lithium Valley. As mentioned, the flow rates from the geothermal recycling process are very high so the extraction methods need to be scaled up for the higher flow rates. While the Smackover play has a much higher lithium concentration than the Salton Sea, it may have a lower brine production rate. I am just speculating here. The Salton Sea has the advantage that the extraction of the metals is a co-benefit to the geothermal power plants so that operation is simultaneous. It is unlikely that existing Smackover oil and gas wells will develop mineral extraction as a co-benefit, especially since standalone brine wells have been the preferred method for bromine recovery for many years. Berkeley Lab has been leading the effort to quantify the Salton Sea geothermal brine resources.

     Flow rates may also affect the depletion of the brine of the desired minerals. Productivity of wells, flow rates and recirculation rates, and geochemistry of the brine are some of the main variables that can affect depletion. The paper about the environmental impacts of DLE from brines emphasized the importance of geochemical heterogeneity as follows: “Knowledge of the precise number, distribution and depths of brine and fresh water wells is vital for hydrogeological modeling of lithium brine deposits. The distinct hydrogeology of each salar means that each deposit should be modelled independently, and results from one exploitation cannot be directly extrapolated to another.” This suggests that there should be more data collected as brine samples at different depths in many more wells to map out mineral concentrations in each zone. This data should be compared to geology trends like faults and stratigraphy.

 

 


 

Brine Mining from Marcellus Shale Produced Water in Pennsylvania

 

     Brine mining projects in the Marcellus Formation in Pennsylvania tap a brine with a lithium concentration of 95mg/L on average but also leverage pre-existing oilfield water treatment facilities where direct mineral extraction provides additional revenue. According to Shale Directories: “Eureka Resources owns and operates three centralized treatment/recycling facilities that process flowback/produced waters (i.e. wastewater) from the Marcellus Shale. Two of the facilities are located in Williamsport (Lycoming County), PA, and one in Standing Stone Township (Bradford County), PA, near Towanda. Eureka has just announced a joint venture to use high tech to recover lithium from the Marcellus wastewater they process.” The lithium recovery venture was announced together with Canada’s MGX Minerals in March 2019. The Eureka process treats about 10,000 Bbls (420,000 gals) per day of brine to extract sodium chloride, calcium chloride, freshwater, and lithium. MQX Minerals uses its own DLE method to extract lithium. Together the two companies plan to install multiple lithium rapid recovery systems at wastewater treatment facilities across the Marcellus and Utica shale formations. Utica brine has a lower average lithium, around 70mg/L which is near the cutoff of economic feasibility. This effort opened the gates to petrolithium, the extraction of lithium from oilfield brines. They say they can process oilfield brines rapidly and at smaller scales as well.

     In November 2020 Eureka Resources got a patent for their own lithium extraction technology and expanded their Northeast Pennsylvania operations. Eureka reported in late July 2023 that they successfully produced 97% pure lithium carbonate from the Marcellus brine, in partnership with SEP Salt & Evaporation Plants Ltd. (SEP). Apparently, they are utilizing the same methods to extract lithium as they use to extract sodium chloride and calcium chloride. They say it will be operational within two years, by mid-2025, which would make it the fastest-to-market lithium brine extraction technology, including DLE (it is apparently not a DLE method as normally understood). The brine is pretreated to remove heavy metals, ammonia, magnesium, sulfates, carbonates, and TOC through filtration, pH adjustment and precipitation reactions. SEP employs several proprietary extraction and recrystallization processes.

      Below is a process schematic for the solvent extraction method tested on Marcellus brine.




Solvent extraction method for lithium recovery from diluted shale gas produced water utilizing D2EHPA as the extractant in Marcellus brine. Source: Lithium recovery from brine: Recent developments and challenges. Abdullah Khalil, Shabin Mohammed, Raed Hashaikeh, Nidal Hilal. Desalination. Volume 528, 15 April 2022, 115611. Lithium recovery from brine: Recent developments and challenges - ScienceDirect


Oilfield Brines Processing. Source SEP





Source: SEP

 



Paradox Basin Brine Mining Play in Utah and Colorado: Lithium, Potash, Bromine, and Boron

      The Paradox Basin is a Pennsylvanian-aged sedimentary basin with a thick sequence of evaporites and brines that yield favorable concentrations of minerals. It is thought to be one of the largest potential sources of potash in America. The brines also contain commercial concentrations of lithium, bromine, boron, and likely iodine. The depths of the brines in the Southern Natural Gas well log and stratigraphic column (shown below) range from 5000ft to 7500ft below the surface. American Potash Corporation is exploring for brine minerals in the Paradox Basin and expects to employ both solar evaporation ponds and direct extraction.  








     Anson Resources plans to extract lithium and bromine from Paradox Basin brines in Utah. According to Mining Weekly: “The proposed Phase 2 expansion will target substantial expansion in the production of lithium carbonate and bromine, and will expand the Paradox project resources through the re-entry and sampling of historic wells, including Mineral Canyon; Sunburst; and high-grade, large Mississippian formations.” Thus, they plan to get more concentration data, including for deeper Mississippian formations.


 





Brine Processing Plants Processing Oilfield Brines and Desalinization Plant Effluent for Minerals Extraction, Irrigation, and Drinking Water

     A Brine processing plant plans to extract minerals from oilfield brine and brackish brine from the adjacent desalinization plant. This is not happening anywhere yet but a project in El Paso, Texas, that previously failed to materialize due to financial, investor, and engineering difficulties was purchased by a Florida company, Critical Minerals Corporation that plans to reconfigure and run the plant. The desalinization plant, the largest inland one in the U.S., has been in operation since 2007. The plan is to treat the brine and extract minerals to sell to oil & gas companies and for fertilizer. Lithium extraction is also in the works when more lithium-rich brines can be delivered. The brine processing plant will be the first of its kind in the country. I am not sure about the timeline or what stage of commercialization is happening at present.  

 

Japanese Iodine-Rich Brine and Natural Gas Play

     Chile produces more than half of the world’s iodine and Japan about 30%. Together the two countries produce nearly 90% of the global supply. Chile’s production comes from naturally concentrated precipitates. Japan produces iodine along with natural gas from brines. Natural gas is dissolved in the brines in Chiba prefecture and other areas. According to the book Iodine Chemistry and Applications: “Iodine production in Japan occurs at the Minami-Kanto gas field near Tokyo, the Niigata gas field, the Nakajo oil and gas field, both in Niigata Prefecture, and the Sadowara gas field in Miyazaki Prefecture, all of which are brine-dissolved gas fields. Although iodine is known to exist at high concentrations in submarine sediments, the commercial production of iodine from brine involves drilling on land. In Japan, iodine is produced from natural gas brine by a blowing-out process and an ion-exchange process.” After extraction, the water must be reinjected back into the ground to prevent land subsidence due to the presence of unconsolidated sediments. This prevents the operations from expanding processing volumes. Below is a schematic of the blowout process for extracting iodine.


 


Blow Out Method Used to Extract Iodine from Japanese Brines


Iodine Brine Play in Pennsylvanian Morrow Sandstone in the Anadarko Basin in Northwest Oklahoma

     The U.S. is the world’s third-largest iodine producer. The iodine in the U.S. comes from the Late Pennsylvanian-aged Morrow Sandstone in the Anadarko Basin of Northwest Oklahoma. AAPG’s Susan Nash writes “Chile is the world’s dominant producer, where iodine is recovered principally by heap-leaching nitrates containing iodate. In Japan’s Chiba prefecture, iodine is recovered from natural gas brines using the blowing out process, which involves vaporizing the iodine, then absorbed, crystallized, and purified. In Oklahoma, the iodine is found in the Morrow sand brines. It is also extracted via proprietary processes from the oilfield brines co-produced with oil and gas. There are currently three operators in Oklahoma, along with another chemical company that creates products from the brine.” The iodine-rich brine is produced from a single paleo-valley located in the Anadarko Basin in one specific feature, the Woodward Trench, a paleo-valley 1 to 2 miles wide in the Morrow formation that extends 70 miles from Vici, Oklahoma, north to the Kansas border. The source of the iodine is the Late Devonian/Early Mississippian Woodford Shale which lies below the Morrow. Organic matter including seaweed, brown algae, coral, and other marine life helped to concentrate the iodine in the shale. The iodine concentration in the Mississippian rocks of the Woodward Shale is as high as 1560 parts per million (ppm). The iodine-rich brines occur at depths from 6000 ft to 10,000 ft below the surface. The iodine concentration in the Morrow Sandstone is as high as 700 ppm. This is about twice as concentrated as the Japanese brines which have average concentrations of about 160 mg/L. This maximum concentration (700 ppm) is at least three times higher than anywhere else found in the U.S. with the exception of newly found iodine-rich brines in the Paradox Basin with concentrations as high as 596mg/L, almost twice that of the Morrow Sand.  Nash wonders whether there are any other paleo valleys in the Anadarko vicinity or elsewhere with iodine-rich brine that await discovery.







     The first iodine processing plant was built in Oklahoma in 1977, based on Japanese and European designs. Acids are used in iodine processing, which requires precautions for handling corrosive material. Iodine prices rose sharply in 2017-2023 by 200%. Uses for iodine include X-ray contrast (biggest use), disinfectants, liquid crystal displays (LCDs), nutritional supplements for humans and animals, pharmaceuticals, LEDs, and specialty chemicals. Iodine recovery from oilfield brines involves settling tanks where the oil is skimmed off the top and chlorination of the brine which separates out the iodine. The vaporized iodine compounds are condensed back into a liquid or solid form through distillation or sublimation and further purified by extraction through oxidation-reduction reactions. The process yields flakes or pellets of 98% pure iodine.

 


This map does not have the 596mg/L data point in Southeast Utah Paradox Basin


Leduc Lithium Brine Play in Western Canada

     E3 Lithium reported in mid-October 2023 that they recently tested their DLE pilot project in Alberta’s Leduc Brines. The tests evaluated lithium recovery and lithium grade at different flow rates. The company noted that all the parameters exceeded their expectations. Thus, they are optimistic about continuing toward commercialization. The Leduc brines are at the lower end of lithium concentrations for economic viability so I would guess projects in that range would be especially sensitive to lithium prices and things like O&M costs.

     Calgary, Alberta-based Volt Lithium has a pilot demo project at Rainbow Lake in northwest Alberta. They are processing oilfield brines from throughout North America. Lithium hydroxide and lithium carbonate are produced. The pilot was a success. They are now building a permanent demonstration plant. A schematic is shown below.





Extraction of Rare Earth Elements from Brines: Currently, Not Economically Feasible

     A 2017 paper On the Extraction of Rare Earth Elements from Geothermal Brines. York R. Smith, Pankaj Kumar, and John D. McLennan. Resources 2017, 6(3), 39, concluded that “rare earth element extraction from geothermal fluids is technically possible, but neither economically viable nor strategically significant at this time.” Rare earths can far better be extracted from veins of much higher concentration than brines. Basically, the same separation methods used for critical minerals would be used to separate rare earth elements in brines, if and when doing so ever becomes feasible.

 




Market Predictions and Incentives

     Most economic scenarios that incorporate the energy transition forecast continued increases in demand for lithium and some of the other brine minerals. DLE as a processing method is very desirable due to its low environmental, climate, and land footprints. It is already modeled as cost-comparable to solar evaporation. Thus, it seems likely that widespread adoption is likely in the next 5-10 years. The number of pilot and commercialization projects in development and planning has been growing. Over the next 2-5 years we should get an idea of what DLE can do to meet demand and for the U.S. perhaps ensure a more robust domestic supply with clean energy credentials.

     In the U.S. the Critical Minerals Exploration Tax Credit (CMETC) was expanded from 15% to 30% as part of the Inflation Reduction Act. This credit includes lithium and a few other brine minerals like zinc and magnesium. It will offset some of the inflation and help companies commercialize their projects and operations.

 

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Iodine. Stanley T. Krukowski. Oklahoma Geological Survey. Mining Engineering. July 2016. MEV68.7P54-57-Krukowski-Iodine.pdf (ou.edu)

Engineering Li/Na selectivity in 12-Crown-4–functionalized polymer membranes. Samuel J. Warnock, Rahul Sujanani, Everett S. Zofchak, and Christopher M. Bates. PNAS. September 7, 2021 118(37). Engineering Li/Na selectivity in 12-Crown-4–functionalized polymer membranes | PNAS

How lithium can be efficiently extracted from oil and gas wastewater. Mining.Com. Staff Writer | September 22, 2021. How lithium can be efficiently extracted from oil and gas wastewater - MINING.COM

On the Extraction of Rare Earth Elements from Geothermal Brines. York R. Smith, Pankaj Kumar, and John D. McLennan. Resources 2017, 6(3), 39. Resources | Free Full-Text | On the Extraction of Rare Earth Elements from Geothermal Brines (mdpi.com)

Eureka Resources expanding operations in northeast Pennsylvania. NCPA Staff Mar 29, 2021. North Central PA. Eureka Resources expanding operations in northeast Pennsylvania | Business | northcentralpa.com

Eureka Resources Successfully Produces Lithium Carbonate From Oil & Natural Gas Brine Wastewater. July 31, 2023. Business Wire. Eureka Resources Successfully Produces Lithium Carbonate From Oil & Natural Gas Brine Wastewater | Business Wire

Shale Gas Produced Water. SEP. Shale Gas Produced Water (sepwin.ch)

Lithium Salts. SEP. Lithium Salts (sepwin.ch)

Paradox basin brine project. US. Sheila Barradas. Creamer Media’s Mining Weekly. May 12. 2023. Paradox basin brine project. US (miningweekly.com)

Utica Shale Play Oil and Gas Brines: Geochemistry and Factors Influencing Wastewater Management. Madalyn S. Blondes, Jenna L. Shelton, Mark A. Engle, Jason P. Trembly, Colin A. Doolan, Aaron M. Jubb, Jessica C. Chenault, Elisabeth L. Rowan, Ralph J. Haefner, and Brian E. Mailot. Environ. Sci. Technol. 2020, 54, 21, 13917–13925. October 14, 2020. Utica Shale Play Oil and Gas Brines: Geochemistry and Factors Influencing Wastewater Management | Environmental Science & Technology (acs.org)

Berkeley Lab leading investigation to quantify and characterize Salton Sea’s geothermal lithium resources. Green Car Congress. February 17, 2022. Berkeley Lab leading investigation to quantify and characterize Salton Sea’s geothermal lithium resources - Green Car Congress

Iodine and Natural Gas. Nippoh Chemicals. Iodine and Natural Gas | Unique Technologies | NIPPOH CHEMICALS (npckk.co.jp)

Iodine Chemistry and Applications, Editor: Tatsuo Kaiho, Wiley, October 2014. Chapter 13: Iodine Production from Natural Gas Brine. Iodine Production from Natural Gas Brine - Iodine Chemistry and Applications - Wiley Online Library

 









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